Code No: 07A70808

R07

Set No. 2

1. Discuss about:

ld .

(a) Importance of spinnerets in tubular membrane.

in

IV B.Tech I Semester Examinations,MAY 2011 MEMBRANE TECHNOLOGY Chemical Engineering Time: 3 hours Max Marks: 80 Answer any FIVE Questions All Questions carry equal marks ?????

(b) Explain the laboratory setup for tubular membrane preparation.

(c) Write the methods to prepare hallow fiber and capillary membrane. [6+6+4] 2. Write short note on

or

(a) Resistance towards mass transport.

(b) Concentration polarization in pressure driven membranes. (c) Fully developed laminar and turbulent flow.

[6+4+6]

3. (a) Discuss Henrys law and Langmuir equations.

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(b) Discuss transportation through porous membrane.

4. Discuss DSC/DTA physical methods for non porous membrane.

[8+8] [16]

5. (a) Pressure retarded osmosis(PRO) allows to produce energy originating from an osmotic flow due to an osmotic pressure difference.

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(b) Is the maximum power obtained at ∆p =0?Calculate the power which can be generated from 3% and a 15% NaCl solution respectively, and a membrane permeability of Lp= 0.36 kg/m2 ,hr.bar(assume vont hoff law is still valid) [8+8]

6. (a) Write the uses of plates and frames in plate and frame module. (b) Explain spiral wound module with diagram.

[6+10]

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7. Write short note on: (a) Firkin flux.

(b) porous membranes. (c) Carrier mediated transport.

(d) Facilitated transport.

[4+4+4+4]

1

Code No: 07A70808

R07

Set No. 2

∆p flux(mol/hr) 5 103 10 202 15 287 20 386 25 501

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nt

uW

or

?????

2

[16]

ld .

Determine the water permeability coefficient graphically.

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8. The pure water flux of a membrane with a diameter of 7.5 cm has been determined as a function of the applied pressure. The following results are obtained:

Code No: 07A70808

R07

Set No. 4

1. Compare the different membranes for basic parameters. 2. Discuss clustering and solubility of liquid mixture.

(a) Dip coating (b) Interfacial polymerization. (c) Spray coating.

[16]

[16]

or

(d) Capillary membranes. 4. Explain:

[16]

ld .

3. Define:

in

IV B.Tech I Semester Examinations,MAY 2011 MEMBRANE TECHNOLOGY Chemical Engineering Time: 3 hours Max Marks: 80 Answer any FIVE Questions All Questions carry equal marks ?????

(a) Boundary layer resistance model.

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(b) Gel layer model.

[8+8]

5. Discuss following with diagrammatic representation: (a) Asymmetric membranes. (b) Porous membranes.

(c) Homogeneous membranes.

(d) Cylindrical porous membranes.

[16]

6. Write short note on:

nt

(a) gas separation through non porous membrane.

(b) choice of organic solvents in liquid membrane.

[16]

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7. A polymer solved in a water has a hydrodynamic radius of 15 nm. Calculate the rejection of membrane with a uniform pore radius 0.05 m and 0.1 m for the case of no adsorption at the pore wall and for the case with monolayer adsorption at the pore wall. [16]

8. Calculate the osmotic pressure of the following aqueous solution 3% NaCl(MNacl = 58.45 g/mol) by weight, 3% albumin(Malb 65.000 g/mol) by weight and a suspension containing 30 g/l of a solid (where the particle weight is 1 ng= (10−9 g) at a temperature 25 C. [16] ????? 3

Code No: 07A70808

R07

Set No. 1

in

IV B.Tech I Semester Examinations,MAY 2011 MEMBRANE TECHNOLOGY Chemical Engineering Time: 3 hours Max Marks: 80 Answer any FIVE Questions All Questions carry equal marks ????? 1. (a) Write brief note on consequences of concentration polarization.

ld .

(b) Discuss fully developed laminar and turbulent velocities in a pipe with diagram. [6+10] 2. (a) List out the industrial applications of micro filtration. (b) List out the industrial applications of ultra filtration.

[8+8]

or

3. (a) Write any six physical and chemical properties and give classification based on their separation process. (b) Define separation process and explain the sorting demon process. 4. Explain how to determine diffusion coefficient by time lag method.

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5. Explain and justify:

[8+8] [16]

(a) Importance of membrane structure.

(b) Importance of materials used to prepare synthetic membrane. 6. Discuss about hallo fiber module and plate and frame module.

[16] [16]

7. Draw and explain the following with diagrams: (a) Supported liquid membranes.

[8+8]

8. Discuss wide angle XRD with graph .

[16]

?????

Aj

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(b) Emulsion liquid membranes.

4

Code No: 07A70808

R07

Set No. 3

in

IV B.Tech I Semester Examinations,MAY 2011 MEMBRANE TECHNOLOGY Chemical Engineering Time: 3 hours Max Marks: 80 Answer any FIVE Questions All Questions carry equal marks ????? 1. Discuss briefly about:

ld .

(a) Interactive system. (b) Henrys law. (c) Diffusion coefficient. (d) Flux.

[16]

(a) Plasma etching. (b) Archimedes principle. 3. Discuss about:

or

2. Write notes on:

[8+8]

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(a) Importance of spinnerets in tubular membrane.

(b) Explain the laboratory setup for tubular membrane preparation. (c) Write the methods to prepare hallow fiber and capillary membrane. [6+6+4] 4. (a) Write the important parameters of electro dialysis (b) Explain separation of amino acids through electro dialysis

[8+8]

5. (a) Write a note on modules and process designs.

nt

(b) Discuss about plate and frame modules with schematic flow path.

[6+10]

6. Discuss the following: (a) Membrane.

Aj

(b) Membrane process. (c) Selectivity.

(d) Flow.

[16]

7. (a) Write the concepts of pervaporation. (b) Short note on supported liquid membranes. (c) draw and explain schematic drawing of the pervaporation process with a downstream vacuum. (d) Write a short note on porous membrane. 5

[16]

Code No: 07A70808

R07

Set No. 3

in

8. (a) A 5% solution of sucrose (Mw = 342 g/l) is concentrated using a tubular nano filtration membrane with an internal diameter of 6mm. The membrane shows a complete rejection for sucrose. With a feed solution of 5 wt%, a temperature of 20 C and a pressure of 20 bar, a flux is measured of 33.5 l/m2 .hr at a cross flow velocity of 0.5 m/s while at a velocity 4.5 m/s a flux is measured of 48.9 l/m2 h. other data density is 103 kg/m3 η = 1.1*10−3 pa.S a= 0.05, b= 1.1 Dsucr = 4.2 *10−10 m2 /s. (b) Calculate the concentration polarization modules for both flow rates.

Aj

nt

uW

or

?????

ld .

(c) calculate the flux at 10 bar assuming that the concentration polarization. modules remains same. [16]

6

R07 Set No. 2

Discuss clustering and solubility of liquid mixture. [16] · 3. Define: ... no adsorption at the pore wall and for the case with monolayer adsorption at the · pore wall.

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